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Journal of Bioactive and Compatible Polymers
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Synthesis and Some Properties of Poly(Alkylene Phosphorothioate)s Prepared from the Corresponding Poly(Alkylene H-Phosphonate)s

O. Kuznetsova

Academy of Fine Chemical Technology, Vernadskogo 86, 117571 Moscow, Russia

K. Kaluzynski

Center of Molecular and Macromolecular Studies, Polish Academy of Sciences, 90-363 Lodz, Sienkiewicza 112, Poland

G. Lapienis

Center of Molecular and Macromolecular Studies, Polish Academy of Sciences, 90-363 Lodz, Sienkiewicza 112, Poland

J. Pretula

Center of Molecular and Macromolecular Studies, Polish Academy of Sciences, 90-363 Lodz, Sienkiewicza 112, Poland

S. Penczek

Center of Molecular and Macromolecular Studies, Polish Academy of Sciences, 90-363 Lodz, Sienkiewicza 112, Poland

Several high molecular weight poly(alkylene phosphorothioate)s were synthesized by reacting poly(H-phosphonate)s with sulfur. The molecular weight of the resulting polymers are similar to the respective starting poly(alkylene H-phosphonate)s indicating that during sulfurization process no chain degradation occurred. The structure of poly(alkylene phosphorothioate)s was confirmed by the analysis of 1H, 13C and 31P NMR spectra.

Journal of Bioactive and Compatible Polymers, Vol. 14, No. 3, 232-242 (1999)
DOI: 10.1177/088391159901400303


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